6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate
CAS No.:1383449-98-6
Molecular Formula:C₂₉H₂₉Cl₃N₄O₅
Molecular Weight:619.932
Hs Code.:

Synonyms:6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of 6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

Chemical Property:

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Technology Process of 6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

There total 6 articles about 6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 1383449-98-6
6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1016/j.carres.2012.04.005

Reference yield:

: C₂₀H₂₄O₇S₂

: 1383449-98-6
6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide

2: N-Bromosuccinimide / acetone; water

With N-Bromosuccinimide; sodium azide; In water; N,N-dimethyl-formamide; acetone;
DOI:10.3390/md14060116

Reference yield:

: 1152-39-2
p-methylphenyl 1-thio-β-D-glucopyranoside

: 1383449-98-6
6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap

2: sodium azide / N,N-dimethyl-formamide

3: N-Bromosuccinimide / acetone; water

With pyridine; dmap; N-Bromosuccinimide; sodium azide; In water; N,N-dimethyl-formamide; acetone;
DOI:10.3390/md14060116