methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

Base Information

Chemical Name:methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate
CAS No.:913622-66-9
Molecular Formula:C₂₅H₄₃ClO₄Si₂
Molecular Weight:499.238
Hs Code.:

Synonyms:methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

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Technology Process of methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

There total 1 articles about methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 811788-11-1
methyl 2,4-bis(tert-butyldimethylsilanyloxy)-3-chloro-6-methylbenzoate

: 5162-44-7
1-bromo-4-butene

: 913622-66-9
methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; at -40 ℃; for 1h;
DOI:10.1021/jo061054f

Reference yield: 82.0%

: 913622-66-9
methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate

: 913622-67-0
3-chloro-4,6-dihydroxy-2-(pent-4-enyl)benzoic acid

Guidance literature:: methyl 4,6-bis(tert-butyldimethylsilyloxy)-3-chloro-2-(pent-4-enyl)benzoate; With lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 1h;

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium n-propylmercaptide; at 20 ℃; for 2.5h;
DOI:10.1021/jo061054f