Technology Process of C13H11BrClNO2
There total 3 articles about C13H11BrClNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
formic acid-triethylamine complex;
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / acetone / 1 h / 25 °C / Inert atmosphere
2: formic acid-triethylamine complex / (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
With
formic acid-triethylamine complex; caesium carbonate;
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine;
In
N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / acetone / 1 h / 25 °C / Inert atmosphere
2: formic acid-triethylamine complex / (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
With
formic acid-triethylamine complex; caesium carbonate;
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine;
In
N,N-dimethyl-formamide; acetone;