[(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Base Information

• Chemical Name: [(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]
• CAS No.: 769154-34-9
• Molecular Formula: C₃₂H₁₂BF₂₄*C₃₄H₃₅FeNPPdS
• Molecular Weight: 1546.19

Synonyms:[(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Chemical Property of [(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Chemical Property:

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Technology Process of [(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

There total 2 articles about [(C₅H₅)Fe(C₅H₃(S-t-Bu)PPh₂)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

[(1-diphenylphosphanyl-2-t-butylsulfenylferrocene)PdCl(CH3)] (769154-27-0) + benzonitrile (100-47-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [(1-diphenylphosphanyl-2-t-butylsulfenylferrocene)Pd(CH3)(NCPh)] tetrakis(3,5-bis(trifluoromethyl)phenyl)borate (769154-34-9)

Guidance literature:

In dichloromethane; at room temp.;

DOI:10.1002/anie.200460087

Reference yield: 71.0%

((C5H5)Fe(C5H3(SC(CH3)3)P(C6H5)2))PdCl(CH3) (769154-27-0) + benzonitrile (100-47-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [(C5H5)Fe(C5H3(S-t-Bu)PPh2)Pd(Me)(benzonitrile)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] (769154-34-9)

Guidance literature:

In dichloromethane; benzonitrile; byproducts: NaCl; Fe-Pd complex treated with stoich. amt. of NaB(C6H3(CF3)2)4 in CH2Cl2-PhCN; filtered; solvent evapd. from filtrate; triturated with hexanes-Et2O;

DOI:10.1021/ja055692b

upstream raw materials:

[(1-diphenylphosphanyl-2-t-butylsulfenylferrocene)PdCl(CH₃)]

benzonitrile

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

((C₅H₅)Fe(C₅H₃(SC(CH₃)3)P(C₆H₅)2))PdCl(CH₃)

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