4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

Base Information

Chemical Name:4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide
CAS No.:1325238-13-8
Molecular Formula:C₁₆H₂₀N₂O₅
Molecular Weight:320.345
Hs Code.:

Synonyms:4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

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Chemical Property of 4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

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Technology Process of 4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

There total 2 articles about 4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 2459-05-4
(E)-4-ethoxy-4-oxobut-2-enoic acid

: 65734-58-9
2-amino-N-(4-methoxyphenyl)propionamide

: 1325238-13-8
4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

Guidance literature:: (E)-4-ethoxy-4-oxobut-2-enoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

2-amino-N-(4-methoxyphenyl)propionamide; With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1155/2011/403129

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1325238-13-8
4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: trifluoroacetic acid / 2 h / 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With diphenyl phosphoryl azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1155/2011/403129

Reference yield:

: 1325238-13-8
4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide

: 1325238-16-1
3-[1-(4-methoxyphenylcarbamoyl)ethylcarbamoyl]acrylic acid

Guidance literature:: 4-oxopent-2-enoic acid [1-(4-methoxyphenylcarbamoyl)ethyl]amide; With lithium hydroxide; In methanol; water; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1155/2011/403129