C₃₃H₃₈N₆O₄

Base Information

Chemical Name:C₃₃H₃₈N₆O₄
CAS No.:1227160-53-3
Molecular Formula:C₃₃H₃₈N₆O₄
Molecular Weight:582.703
Hs Code.:

C<sub>33</sub>H<sub>38</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₃₃H₃₈N₆O₄

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Chemical Property of C₃₃H₃₈N₆O₄

Chemical Property:

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Technology Process of C₃₃H₃₈N₆O₄

There total 6 articles about C₃₃H₃₈N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1225380-88-0
5-methyl-1-{3-[(4-methylpiperazin-1-yl)carbonyl]benzyl}-1H-pyrazole-3-carboxylic acid

: 1227160-06-6
2-[1-(4-cyanophenyl)cyclobutyl]ethyl acetate

: 1227160-53-3
C₃₃H₃₈N₆O₄

Guidance literature:: 5-methyl-1-{3-[(4-methylpiperazin-1-yl)carbonyl]benzyl}-1H-pyrazole-3-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

2-[1-(4-cyanophenyl)cyclobutyl]ethyl acetate; In N,N-dimethyl-formamide; at 20 - 140 ℃; for 2h;

Reference yield:

: 1225380-89-1
ethyl 1-[3-(tert-butoxycarbonyl)benzyl]-5-methyl-1H-pyrazole-3-carboxylate

: 1227160-53-3
C₃₃H₃₈N₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / Inert atmosphere

2.2: 16 h / 20 °C

3.1: sodium hydroxide / ethanol / 2 h / 70 °C

3.2: pH Ca_.4

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 2 h / 20 - 140 °C

With oxalyl dichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 126062-63-3
1,1-dimethylethyl 3-bromomethylbenzoate

: 1227160-53-3
C₃₃H₃₈N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

3.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / Inert atmosphere

3.2: 16 h / 20 °C

4.1: sodium hydroxide / ethanol / 2 h / 70 °C

4.2: pH Ca_.4

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 2 h / 20 - 140 °C

With oxalyl dichloride; potassium tert-butylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;