4-methylbenzyl benzoylacetate

Base Information

Chemical Name:4-methylbenzyl benzoylacetate
CAS No.:505092-97-7
Molecular Formula:C₁₇H₁₆O₃
Molecular Weight:268.312
Hs Code.:

Synonyms:4-methylbenzyl benzoylacetate

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Chemical Property of 4-methylbenzyl benzoylacetate

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Technology Process of 4-methylbenzyl benzoylacetate

There total 1 articles about 4-methylbenzyl benzoylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-18-4
4-Methylbenzyl alcohol

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 505092-97-7
4-methylbenzyl benzoylacetate

Guidance literature:: In toluene; for 16h; Heating;
DOI:10.1021/jo020453h

Reference yield:

: 505092-97-7
4-methylbenzyl benzoylacetate

: (E)-3-Amino-3-phenyl-acrylic acid 4-methyl-benzyl ester

Guidance literature:: With ammonium acetate; In methanol; at 20 ℃; for 72h;
DOI:10.1021/jo020453h

Reference yield:

: 505092-97-7
4-methylbenzyl benzoylacetate

: 1,3-dimethyl-4-(((4-methylbenzyl)oxy)carbonyl)-2,5-diphenyl-1H-imidazol-3-ium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 17 h / Reflux

2: iodine; dipotassium hydrogenphosphate / 1,2-dichloro-ethane / 3 h / 50 °C

With dipotassium hydrogenphosphate; iodine; acetic acid; In ethanol; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.9b00541