(C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

Base Information

Chemical Name:(C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅
CAS No.:1160697-89-1
Molecular Formula:C₄₁H₄₁N₅
Molecular Weight:603.81
Hs Code.:

(C<sub>5</sub>H<sub>4</sub>N)2C<sub>5</sub>H<sub>2</sub>NC<sub>6</sub>H<sub>4</sub>N(CH<sub>2</sub>)3CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>N(CH<sub>2</sub>)3CH<sub>3</sub>C<sub>6</sub>H<sub>5</sub>

Synonyms:(C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

Suppliers and Price of (C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

There total 1 articles about (C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 109-65-9
1-bromo-butane

: 1160698-18-9
C₃₃H₂₅N₅

: 1160697-89-1
(C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

Guidance literature:: C₃₃H₂₅N₅; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

1-bromo-butane; In tetrahydrofuran; mineral oil; Inert atmosphere; Reflux;
DOI:10.1039/b820392j

Reference yield: 74.0%

: ammonium hexafluorophosphate

: 14898-67-0
ruthenium(III) chloride trihydrate

: 1160697-89-1
(C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅

: Ru((C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅)2⁽²⁺⁾*2PF₆^(1-)=Ru((C₅H₄N)2C₅H₂NC₆H₄N(CH₂)3CH₃C₆H₄N(CH₂)3CH₃C₆H₅)2(PF₆)2

Guidance literature:: With N-ethylmorpholine; In ethanol; water; (under Ar, Schlenk); RuCl3*3H2O and ligand heated at reflux in EtOH contg. N-ethylmorpholine for 12 h, cooled to room temp., aq. soln. of NH4PF6added; silica gel column chromy. with MeCN/sat. aq. KNO3/H2O, collected, vol. reduced in vacuo, treated with aq. NH4PF6, filtered, ppt. redissolved in MeCN with H2O, dried under vac.; elem. anal.;
DOI:10.1039/b820392j