{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

Base Information

Chemical Name:{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine
CAS No.:1256336-62-5
Molecular Formula:C₃₉H₅₆BN₃O₈
Molecular Weight:705.7
Hs Code.:

{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

Synonyms:{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

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Chemical Property of {4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

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Technology Process of {4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

There total 4 articles about {4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1256336-55-6
2-methoxy-3-(2-((4-bromomethyl)-benzoylamino)-2-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6.1.1.0(2,6)]dec-4-yl)-ethyl)-benzoic acid tert-butyl ester

: 1256336-62-5
{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

Guidance literature:: In dichloromethane; at 20 ℃;

Reference yield:

: 913836-10-9
3-(dihydroxyboranyl)-2-methoxybenzoic acid

: 1256336-62-5
{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 1,4-dioxane; water / 18 h / 0 - 20 °C / Sealed tube

2.1: tetrahydrofuran / 1 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / -100 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C / Inert atmosphere

4.2: -100 - 0 °C / Inert atmosphere

4.3: -78 - 20 °C / Inert atmosphere

5.1: dichloromethane / -20 - 20 °C / Inert atmosphere

6.1: dichloromethane / 20 °C

With n-butyllithium; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water;

Reference yield:

: 1155425-67-4
2-methoxy-3-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]dec-4-yl)benzoic acid tert-butyl ester

: 1256336-62-5
{4-[2-(3-tert-butoxycarbonyl-2-methoxy-phenyl)-1-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6,1,1,0(2,6)]dec-4-yl)-ethylcarbamoyl]-benzyl}-2-tert-butoxycarbonylamino-ethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -100 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C / Inert atmosphere

2.2: -100 - 0 °C / Inert atmosphere

2.3: -78 - 20 °C / Inert atmosphere

3.1: dichloromethane / -20 - 20 °C / Inert atmosphere

4.1: dichloromethane / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;