Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]-, ethyl ester
CAS No.:914104-00-0
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:
Mol file:914104-00-0.mol

Synonyms:ethyl 4-{2-[(tert-butoxycarbonyl)amino]ethyl}benzoate

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Chemical Property of Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]-, ethyl ester

Chemical Property:

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Technology Process of Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]-, ethyl ester

There total 3 articles about Benzoic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl]aMino]ethyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 914104-00-0
ethyl 4-{2-[(tert-butoxycarbonyl)amino]ethyl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 1,4-dioxane / 2.5 h / 22 °C

1.2: pH 2 / Cooling

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 22 °C

With potassium carbonate; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 60531-36-4
4-(2-amino-ethyl)-benzoic acid hydrochloride

: 914104-00-0
ethyl 4-{2-[(tert-butoxycarbonyl)amino]ethyl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 1,4-dioxane / 2.5 h / 22 °C

1.2: pH 2 / Cooling

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 22 °C

With potassium carbonate; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;