Technology Process of C23H24F3N3O5S
There total 10 articles about C23H24F3N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water;
Alkaline conditions;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: hydrogenchloride / ethyl acetate / 3.5 h / 20 °C
1.2: 0.08 h
1.3: 0.5 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / Cooling with ice
2.2: 8 h / 20 °C
3.1: lithium borohydride / tetrahydrofuran / 20 °C / Cooling with ice
4.1: Dess-Martin periodane / dichloromethane / 9 h / 20 °C / Cooling with ice
5.1: diethylamino-sulfur trifluoride / dichloromethane / 1.5 h / 20 °C
6.1: palladium(II) hydroxide; hydrogen / ethanol; ethyl acetate / 3.5 h / 20 °C
7.1: triethylamine / dichloromethane / 0.58 h / Cooling with ice
8.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C
9.1: water / Alkaline conditions
With
hydrogenchloride; lithium borohydride; diethylamino-sulfur trifluoride; water; hydrogen; palladium(II) hydroxide; sodium hydride; caesium carbonate; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 0.58 h / Cooling with ice
2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C
3: water / Alkaline conditions
With
water; caesium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;