7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

Base Information

Chemical Name:7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene
CAS No.:68485-78-9
Molecular Formula:C₁₆H₁₆N₂O₆
Molecular Weight:332.313
Hs Code.:

Synonyms:7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

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Chemical Property of 7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

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Technology Process of 7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

There total 2 articles about 7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 20205-48-5
7-azabicyclo<4.2.0>oct-3-en-8-one

: 68485-78-9
7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

Guidance literature:: In benzene;

Reference yield:

: 64370-35-0
p-nitrobenzyl glyoxylate

: 20205-48-5,77003-43-1,77131-40-9,98856-65-6
8-oxo-7-azabicyclo<4.2.0>oct-2-ene

: 68485-78-9
7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

Guidance literature:: In benzene; Heating;

Reference yield:

: 68485-78-9
7-(1-Hydroxy-1-p-nitrobenzyloxycarbonylmethyl)-8-oxo-7-azabicyclo[4,2,0]-oct-3-ene

: 104883-29-6
p-nitrobenzyl 2-(2-oxotetrahydrofuran-3-yl)-3,4-dihydro-2H-pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) thionyl chloride, 2,6-dimethylpyridine, 2.) 2,6-dimethylpyridine / 1.) THF, -20 deg C -> -10 deg C, 2.) dioxane, r.t., overnight

3: 94 percent / sodium borohydride / tetrahydrofuran / 0.12 h / 0 °C

4: 0.009 g / pyridine / 1 h / 0 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; thionyl chloride; In tetrahydrofuran; pyridine;