6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

Base Information

Chemical Name:6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole
CAS No.:1473415-49-4
Molecular Formula:C₁₈H₆ClF₁₃N₂
Molecular Weight:532.691
Hs Code.:

Synonyms:6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

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Chemical Property of 6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

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Technology Process of 6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

There total 3 articles about 6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 375-22-4
heptafluorobutyric Acid

: 1473416-72-6
4-[2,4-bis(trifluoromethyl) phenyl]-5-chlorobenzene-1,2-diamine

: 1473415-49-4
6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

Guidance literature:: at 80 ℃;

Reference yield:

: 1635-61-6
5-chloro-2-nitroaniline

: 1473415-49-4
6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; N-iodo-succinimide / water / 3 h / 50 °C / Inert atmosphere

2: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 95 °C / Inert atmosphere

3: zinc; hydrogenchloride / water; ethanol / 2 h / 90 °C

4: 80 °C

With hydrogenchloride; potassium phosphate; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; zinc; In 1,4-dioxane; ethanol; water;

Reference yield:

: 335349-57-0
2-nitro-4-iodo-5-chloroaniline

: 1473415-49-4
6-[2,4-bis(trifluoromethyl)phenyl]-5-chloro-2-(heptafluoropropyl)-1H-1,3-benzodiazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 95 °C / Inert atmosphere

2: zinc; hydrogenchloride / water; ethanol / 2 h / 90 °C

3: 80 °C

With hydrogenchloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc; In 1,4-dioxane; ethanol; water;