N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine

Base Information

• Chemical Name: N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine
• CAS No.: 527672-96-4
• Molecular Formula: C₃₅H₅₆N₂O₂
• Molecular Weight: 536.842
• Mol file: 527672-96-4.mol

Synonyms:N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine

Chemical Property of N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine

There total 1 articles about N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,4-Diazacycloheptane (505-66-8) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-Butylphenol (96-76-4) → N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine (527672-96-4)

Guidance literature:

In water; for 24h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c5dt03119b

Reference yield: 36.0%

N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine (527672-96-4) + trimethylaluminum (75-24-1) + benzyl alcohol (100-51-6,185532-71-2) → Al(C5H10N2(CH2C6H2(C(CH3)3)2O)2)(OCH2C6H5) (1397696-33-1)

Guidance literature:

In toluene; under Ar; soln. of ligand in toluene heated to 50°C; AlMe3 added slowly; stirred at 50°C for 30 min; heated and stirred at 80°C for 3 h; PhCH2OH (excess) carefully added to hot soln.; stirred at 80°C for 3 h; cooled; recrystd. from toluene-hexane; elem. anal.;

DOI:10.1039/c2nj40300e

upstream raw materials:

1,4-Diazacycloheptane

formaldehyd

2,4-di-tert-Butylphenol

Downstream raw materials:

Al(C₅H₁₀N₂(CH₂C₆H₂(C(CH₃)3)2O)2)(OCH₂C₆H₅)