5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

Base Information

Chemical Name:5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime
CAS No.:1290138-35-0
Molecular Formula:C₁₉H₂₂N₄O₃
Molecular Weight:354.409
Hs Code.:

Synonyms:5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

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Chemical Property of 5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

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Technology Process of 5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

There total 6 articles about 5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1290138-34-9
5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde

: 1290138-35-0
5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 150 ℃; for 0.166667h; microwave irradiation;

Reference yield:

: 3471-32-7
4-Methoxyphenylhydrazine

: 1290138-35-0
5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / acetic acid / 30 h / 120 °C

2.1: phosphorus tribromide / acetonitrile / 0.67 h / 150 °C / microwave irradiation

3.1: potassium carbonate; sodium iodide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.33 h / 150 °C / Inert atmosphere; microwave irradiation

4.1: trichlorophosphate / toluene / 0.08 h / 0 °C

4.2: 0.33 h / 150 °C / microwave irradiation

5.1: hydroxylamine hydrochloride; pyridine / ethanol / 0.17 h / 150 °C / microwave irradiation

With pyridine; hydroxylamine hydrochloride; phosphorus tribromide; potassium carbonate; triethylamine; sodium iodide; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; acetic acid; toluene; acetonitrile;

Reference yield:

: 3249-68-1
ethyl butyroyl acetate

: 1290138-35-0
5-(3,5-dimethylisoxazol-4-yl)-1-(4-methoxyphenyl)-3-propyl-1H-pyrazole-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / acetic acid / 30 h / 120 °C

2.1: phosphorus tribromide / acetonitrile / 0.67 h / 150 °C / microwave irradiation

3.1: potassium carbonate; sodium iodide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.33 h / 150 °C / Inert atmosphere; microwave irradiation

4.1: trichlorophosphate / toluene / 0.08 h / 0 °C

4.2: 0.33 h / 150 °C / microwave irradiation

5.1: hydroxylamine hydrochloride; pyridine / ethanol / 0.17 h / 150 °C / microwave irradiation

With pyridine; hydroxylamine hydrochloride; phosphorus tribromide; potassium carbonate; triethylamine; sodium iodide; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; acetic acid; toluene; acetonitrile;