Ethyl 2,6-diethoxybenzoate

Base Information

Chemical Name:Ethyl 2,6-diethoxybenzoate
CAS No.:92157-15-8
Molecular Formula:C13H18 O4
Molecular Weight:238.28
Hs Code.:
DSSTox Substance ID:DTXSID70408014
Wikidata:Q82213371
Mol file:92157-15-8.mol

Synonyms:Ethyl 2,6-diethoxybenzoate;92157-15-8;DTXSID70408014;Ethyl-2,6-diethoxybenzoate,97%;Ethyl 2,6-diethoxybenzoate, 97%;AKOS015889039

Suppliers and Price of Ethyl 2,6-diethoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Ethyl 2,6-diethoxybenzoate 97%
5g
$ 101.00

Sigma-Aldrich
Ethyl 2,6-diethoxybenzoate 97%
1g
$ 28.30

American Custom Chemicals Corporation
ETHYL 2,6-DIETHOXYBENZOATE 95.00%
5G
$ 894.29

American Custom Chemicals Corporation
ETHYL 2,6-DIETHOXYBENZOATE 95.00%
1G
$ 634.15

Total 4 raw suppliers

Chemical Property of Ethyl 2,6-diethoxybenzoate

Chemical Property:

Vapor Pressure:8.58E-05mmHg at 25°C
Melting Point:52-56 °C(lit.)
Refractive Index:1.492
Boiling Point:340.5°C at 760 mmHg
Flash Point:175 °F
PSA：44.76000
Density:1.059g/cm³
LogP:2.66070
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:238.12050905
Heavy Atom Count:17
Complexity:216

Purity/Quality:

97% ^*data from raw suppliers

Ethyl 2,6-diethoxybenzoate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=C(C(=CC=C1)OCC)C(=O)OCC

Technology Process of Ethyl 2,6-diethoxybenzoate

There total 2 articles about Ethyl 2,6-diethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74-96-4
ethyl bromide

: 303-07-1
2,6-Dihydroxybenzoic acid

: 92157-15-8
2,6-Diaethoxy-benzoesaeure-aethylester

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 140 ℃; for 24h;
DOI:10.1021/jm00353a003

Reference yield:

: 92157-15-8
2,6-Diaethoxy-benzoesaeure-aethylester

Guidance literature:: Resorcin, 1)KOH, Xylol, Δ, 2) CO2, DMF, 150-155grad, 3) Aethylsulfat, K2CO3, Acn., Siedetemp.;

Reference yield:

: 92157-15-8
2,6-Diaethoxy-benzoesaeure-aethylester

: 3-Chloro-2,6-diethoxy-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: water, KOH / butan-1-ol / 4 h / Heating

2: 83 percent / SO₂Cl₂ / CHCl₃ / 0.5 h / 50 °C

3: SOCl₂ / toluene / 1 h / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; water; In chloroform; toluene; butan-1-ol;
DOI:10.1021/jm00353a003