(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

Base Information

Chemical Name:(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate
CAS No.:1256386-08-9
Molecular Formula:C₂₄H₃₆N₂O₈
Molecular Weight:480.558
Hs Code.:

Synonyms:(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

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Chemical Property of (R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

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Technology Process of (R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

There total 1 articles about (R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1256386-07-8
(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1256386-08-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 42h;

Reference yield: 59.0%

: 1256386-08-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: 784156-34-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-oxopentanoate

Guidance literature:: (R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate; With lithium tri-t-butoxyaluminum hydride; In diethyl ether; at 20 ℃; for 2h;

With potassium hydrogensulfate; In diethyl ether; water;

Reference yield:

: 1256386-08-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: C₃₃H₄₁N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: lithium tri-t-butoxyaluminum hydride / diethyl ether / 2 h / 20 °C

2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 20 °C / Iinert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With sodium tris(acetoxy)borohydride; lithium tri-t-butoxyaluminum hydride; triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; 1,2-dichloro-ethane;