(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

Base Information

Chemical Name:(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate
CAS No.:1310382-07-0
Molecular Formula:C₄₃H₅₇N₃O₁₀
Molecular Weight:775.94
Hs Code.:

Synonyms:(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

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Chemical Property of (S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

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Technology Process of (S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

There total 3 articles about (S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 784156-34-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-oxopentanoate

: 24458-14-8
Lys(Z)-OBzl

: 1310382-07-0
(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

Guidance literature:: With sodium tris(acetoxy)borohydride; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; Iinert atmosphere;

Reference yield:

: 1256386-07-8
(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: 1310382-07-0
(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / acetonitrile / 42 h / 20 °C

2: lithium tri-t-butoxyaluminum hydride / diethyl ether / 2 h / 20 °C

3: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 20 °C / Iinert atmosphere

With dmap; sodium tris(acetoxy)borohydride; lithium tri-t-butoxyaluminum hydride; triethylamine; In diethyl ether; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1256386-08-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: 1310382-07-0
(S)-benzyl 2-({(R)-5-(benzyloxy)-4-[bis(tert-butoxycarbonyl)amino]-5-oxopentyl}amino)-6-benzyloxycarbonylaminohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium tri-t-butoxyaluminum hydride / diethyl ether / 2 h / 20 °C

2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 20 °C / Iinert atmosphere

With sodium tris(acetoxy)borohydride; lithium tri-t-butoxyaluminum hydride; triethylamine; In diethyl ether; 1,2-dichloro-ethane;