(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

Base Information

Chemical Name:(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate
CAS No.:1256386-07-8
Molecular Formula:C₁₉H₂₈N₂O₆
Molecular Weight:380.441
Hs Code.:

Synonyms:(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

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Chemical Property of (R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

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Technology Process of (R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

There total 1 articles about (R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 34404-30-3
N-(tert-butoxycarbonyl)-D-glutamic acid 1-benzyl ester

: 1256386-07-8
(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

Guidance literature:: N-(tert-butoxycarbonyl)-D-glutamic acid 1-benzyl ester; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;

N,O-dimethylhydroxylamine*hydrochloride; With triethylamine; In dichloromethane;

Reference yield: 79.0%

: 1256386-07-8
(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1256386-08-9
(R)-benzyl 2-[bis(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 42h;

Reference yield:

: 1256386-07-8
(R)-benzyl 2-[(tert-butoxycarbonyl)amino]-5-[methoxy(methyl)amino]-5-oxopentanoate

: C₃₃H₄₁N₃O₆

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / acetonitrile / 42 h / 20 °C

2: lithium tri-t-butoxyaluminum hydride / diethyl ether / 2 h / 20 °C

3: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 20 °C / Iinert atmosphere

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With dmap; sodium tris(acetoxy)borohydride; lithium tri-t-butoxyaluminum hydride; triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; 1,2-dichloro-ethane; acetonitrile;