N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

Base Information

Chemical Name:N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester
CAS No.:158817-12-0
Molecular Formula:C₅₄H₅₆NO₈PSi₂
Molecular Weight:934.185
Hs Code.:

N<sup>α</sup>-(benzyloxycarbonyl)-O-<bis<2-(methyldiphenylsilyl)ethyl>phosphono>tyrosine benzyl ester

Synonyms:N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

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Chemical Property of N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

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Technology Process of N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

There total 5 articles about N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Benzyloxycarbonylamino-3-(4-{bis-[2-(methyl-diphenyl-silanyl)-ethoxy]-phosphanyloxy}-phenyl)-propionic acid benzyl ester

: 158817-12-0
N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

Guidance literature:: With tert.-butylhydroperoxide; In tetrahydrofuran; at 0 ℃; for 2h; Yield given;
DOI:10.1021/jo00101a029

Reference yield:

: 144-79-6
chloromethyldiphenylsilane

: 158817-12-0
N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) LDA / 1.) THF, -78 deg C, 1 h, 2.) r.t., overnight

2: LiAlH₄ / diethyl ether / 1.) r.t., 1 h, 2.) reflux, 2 h

3: 90 percent / Et₃N / diethyl ether / Ambient temperature

4: tetrazole / tetrahydrofuran / 2 h / Ambient temperature

5: 90percent t-BuOOH / tetrahydrofuran / 2 h / 0 °C

With 1H-tetrazole; tert.-butylhydroperoxide; lithium aluminium tetrahydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00101a029

Reference yield:

: 40438-48-0
diphenylmethylsilylethylethanol

: 158817-12-0
N^α-(benzyloxycarbonyl)-O-phosphono>tyrosine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Et₃N / diethyl ether / Ambient temperature

2: tetrazole / tetrahydrofuran / 2 h / Ambient temperature

3: 90percent t-BuOOH / tetrahydrofuran / 2 h / 0 °C

With 1H-tetrazole; tert.-butylhydroperoxide; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00101a029