S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

Base Information

Chemical Name:S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate
CAS No.:169137-58-0
Molecular Formula:C₂₂H₃₀O₃SSi
Molecular Weight:402.63
Hs Code.:

Synonyms:S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

Suppliers and Price of S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

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Technology Process of S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

There total 2 articles about S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-hydroxy-3-phenylpropanethioate

: 333-27-7
methyl trifluoromethanesulfonate

: 169137-58-0
S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

Guidance literature:: With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; In dichloromethane; at -78 ℃; for 2.5h;

Reference yield:

: 124-41-4
sodium methylate

: 169137-45-5
(Z,3R)-3-tert-butyldimethylsiloxy-1-nitro-3-phenyl-1-phenylsulfanylpropene

: 169137-58-0
S-phenyl (2S,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

: S-phenyl (2R,3R)-3-tert-butyldimethylsiloxy-2-methoxy-3-phenylpropanethioate

Guidance literature:: With ozone; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) DMF, MeOH, -45 deg C, 2 h, 2.) -78 deg C;