2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

Base Information

Chemical Name:2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole
CAS No.:1379799-59-3
Molecular Formula:C₂₆H₂₇BrN₂O₃S
Molecular Weight:527.482
Hs Code.:

Synonyms:2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

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Chemical Property of 2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

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Technology Process of 2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

There total 3 articles about 2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5405-34-5
(Z)-2-bromobut-2-enoic acid

: 1379799-58-2
C₂₂H₂₄N₂O₂S

: 1379799-59-3
2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 60h; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.022

Reference yield:

: C₁₉H₁₈N₂O₂S

: 1379799-59-3
2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / -78 - 20 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 60 h / 20 °C / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2012.04.022

Reference yield:

: 752212-01-4
2-allyl-1-(phenylsulfonyl)-3-indolecarbaldehyde

: 1379799-59-3
2-allyl-3-[(Z)-1-(N-methyl-2-bromobut-2-enamido)-3-butenyl]-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / ethanol; dichloromethane / 20 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / -78 - 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 60 h / 20 °C / Inert atmosphere

With acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.tet.2012.04.022