C₄₃H₅₈O₁₀Si

Base Information

Chemical Name:C₄₃H₅₈O₁₀Si
CAS No.:1361049-83-3
Molecular Formula:C₄₃H₅₈O₁₀Si
Molecular Weight:763.013
Hs Code.:

C<sub>43</sub>H<sub>58</sub>O<sub>10</sub>Si

Synonyms:C₄₃H₅₈O₁₀Si

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Chemical Property of C₄₃H₅₈O₁₀Si

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Technology Process of C₄₃H₅₈O₁₀Si

There total 14 articles about C₄₃H₅₈O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1361049-67-3
C₄₇H₆₃ClO₁₁Si

: 1361049-83-3
C₄₃H₅₈O₁₀Si

Guidance literature:: With methanol; potassium carbonate; In tetrahydrofuran;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-71-9
C₁₆H₂₆O₆Si

: 1361049-83-3
C₄₃H₅₈O₁₀Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

1.2: 21 h / 20 °C

2.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

3.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

3.2: 0.5 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

5.1: acetone; acetonitrile / 2 h / Irradiation

5.2: 16 h / 20 °C / 760.05 Torr

6.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

7.1: tetrahydrofuran; diethyl ether / -78 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; sodium hydride; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-60-6
methyl (3R,5R)-5-(tert-butyldimethylsilyloxy)-3-hydroxy-6-heptenoate

: 1361049-83-3
C₄₃H₅₈O₁₀Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 19 h / -78 - 20 °C

1.3: 21 h / -78 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

2.2: 21 h / 20 °C

3.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

4.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

4.2: 0.5 h / 0 °C

5.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

6.1: acetone; acetonitrile / 2 h / Irradiation

6.2: 16 h / 20 °C / 760.05 Torr

7.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

8.1: tetrahydrofuran; diethyl ether / -78 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; sodium hydride; triethylamine; methyl chloroformate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889