phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

Base Information

Chemical Name:phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate
CAS No.:1402585-90-3
Molecular Formula:C₁₆H₁₆FNO₄
Molecular Weight:305.306
Hs Code.:

Synonyms:phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

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Chemical Property of phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

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Technology Process of phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

There total 4 articles about phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1402585-89-0
dimethyl 2-(2-fluoro-4-(phenoxycarbonylamino)phenyl)malonate

: 1402585-90-3
phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

Guidance literature:: With sodium tetrahydroborate; ethanol; lithium chloride; In tetrahydrofuran; at 0 ℃; for 5h;

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 1402585-90-3
phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 50 °C

1.2: 5 h / 50 °C

2.1: hydrogen; palladium 10% on activated carbon / ethanol / 2 h / 23 °C

3.1: pyridine / acetone / 1 h / 0 - 23 °C

4.1: sodium tetrahydroborate; lithium chloride; ethanol / tetrahydrofuran / 5 h / 0 °C

With pyridine; sodium tetrahydroborate; ethanol; palladium 10% on activated carbon; hydrogen; potassium carbonate; lithium chloride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 188975-47-5
dimethyl 2-(2-fluoro-4-nitrophenyl)malonate

: 1402585-90-3
phenyl 4-(1,3-dihydroxypropan-2-yl)-3-fluorophenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 2 h / 23 °C

2: pyridine / acetone / 1 h / 0 - 23 °C

3: sodium tetrahydroborate; lithium chloride; ethanol / tetrahydrofuran / 5 h / 0 °C

With pyridine; sodium tetrahydroborate; ethanol; palladium 10% on activated carbon; hydrogen; lithium chloride; In tetrahydrofuran; ethanol; acetone;