2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

Base Information

Chemical Name:2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone
CAS No.:84755-36-2
Molecular Formula:C₂₇H₂₆O₆
Molecular Weight:446.5
Hs Code.:

Synonyms:2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

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Chemical Property of 2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

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Technology Process of 2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

There total 7 articles about 2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 142836-53-1
2-(4-benzyloxy-3-methoxybenzyl)-3-(3,4-methylenedioxybenzoylpropane-1,3-dithiane)-γ-butyrolactone

: 84755-36-2
2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

Guidance literature:: With Raney nickel W-2; In ethanol; for 4h; Heating;

Reference yield:

: 80483-34-7
4-(1,3-benzodioxol-5-ylmethyl)-4,5-dihydrofuran-2(3H)-one

: 72724-00-6
1-(benzyloxy)-4-(bromomethyl)-2-methoxybenzene

: 84755-36-2
2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 30 min, 2.) THF, a) -20 deg C, 30 min, b) RT, 1 h;
DOI:10.1071/CH9822175

Reference yield:

: 33693-48-0
4-benzyloxy-3-methoxybenzyl alcohol

: 84755-36-2
2-(4-benzyloxy-3-methyoxybenzyl)-3-(3,4-methylenedioxybenzyl)-γ-butyrolactone

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / phosphorus tribromide, Et₃N / CCl₄ / 0 °C

2: 1.) n-butyllitlium

3: 77 percent / Raney nickel W-2 / ethanol / 4 h / Heating

With n-butyllithium; Raney nickel W-2; phosphorus tribromide; triethylamine; In tetrachloromethane; ethanol;