1--6-(benzyloxycarbonylamino)hexane

Base Information

Chemical Name:1--6-(benzyloxycarbonylamino)hexane
CAS No.:85838-37-5
Molecular Formula:C₂₂H₃₃N₃O₆S
Molecular Weight:467.587
Hs Code.:

1-<N-acetyl-S-(carboxymethyl)-DL-homocysteinylamino>-6-(benzyloxycarbonylamino)hexane

Synonyms:1--6-(benzyloxycarbonylamino)hexane

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Chemical Property of 1--6-(benzyloxycarbonylamino)hexane

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Technology Process of 1--6-(benzyloxycarbonylamino)hexane

There total 4 articles about 1--6-(benzyloxycarbonylamino)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 64-69-7
Iodoacetic acid

: 85838-36-4
1-(N-acetyl-DL-homocysteinylamino)-6-(benzyloxycarbonylamino)hexane

: 85838-37-5
1--6-(benzyloxycarbonylamino)hexane

Guidance literature:: With lead acetate; In ethanol; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(83)88217-2

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 85838-37-5
1--6-(benzyloxycarbonylamino)hexane

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / 1.) 12 M HCl; 2.) HCl / 1.) methanol, 18 h; 2.) dichloromethane, 0 deg C

2: 51 percent / triethylamine / ethanol / 4 h

3: 85 percent / lead acetate trihydrate / aq. ethanol / 4 h / Ambient temperature

With hydrogenchloride; lead acetate; triethylamine; In ethanol;
DOI:10.1016/0008-6215(83)88217-2

Reference yield:

: 78618-06-1
monobenzyloxycarbonyl hexamethylenediamine hydrochloride

: 85838-37-5
1--6-(benzyloxycarbonylamino)hexane

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / triethylamine / ethanol / 4 h

2: 85 percent / lead acetate trihydrate / aq. ethanol / 4 h / Ambient temperature

With lead acetate; triethylamine; In ethanol;
DOI:10.1016/0008-6215(83)88217-2