C₅₆H₆₁Cl₆NO₁₆

Base Information

Chemical Name:C₅₆H₆₁Cl₆NO₁₆
CAS No.:1053738-36-5
Molecular Formula:C₅₆H₆₁Cl₆NO₁₆
Molecular Weight:1216.82
Hs Code.:

C<sub>56</sub>H<sub>61</sub>Cl<sub>6</sub>NO<sub>16</sub>

Synonyms:C₅₆H₆₁Cl₆NO₁₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₆H₆₁Cl₆NO₁₆

Chemical Property:

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Technology Process of C₅₆H₆₁Cl₆NO₁₆

There total 8 articles about C₅₆H₆₁Cl₆NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1053738-36-5
C₅₆H₆₁Cl₆NO₁₆

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / HCOOH / methanol; H₂O / 21 h / 20 °C

2: 100 percent / K₂CO₃ / tetrahydrofuran / 12 h / Heating

3: 1.) LiN(Si(CH₃)3)2 / 1.) THF, -78 deg C, 1 h, 2.) -78 deg C, 15 min

4: 70 percent / LiOH, H₂O₂ / tetrahydrofuran; H₂O / 15 h / 20 °C

5: 1.) DCC, 2.) DMAP / 1.) toluene, 20 deg C, 5 min, 2.) 20 deg C, 20 h

With dmap; lithium hydroxide; formic acid; dihydrogen peroxide; potassium carbonate; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00085a004

Reference yield:

: 19810-31-2
Benzyloxyacetyl chloride

: 1053738-36-5
C₅₆H₆₁Cl₆NO₁₆

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / NaH / toluene / 1.) 0 deg C, 30 min, 2.) 20 deg C, 2 h

2: 1.) LiN(Si(CH₃)3)2 / 1.) THF, -78 deg C, 1 h, 2.) -78 deg C, 15 min

3: 70 percent / LiOH, H₂O₂ / tetrahydrofuran; H₂O / 15 h / 20 °C

4: 1.) DCC, 2.) DMAP / 1.) toluene, 20 deg C, 5 min, 2.) 20 deg C, 20 h

With dmap; lithium hydroxide; dihydrogen peroxide; sodium hydride; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; In tetrahydrofuran; water; toluene;
DOI:10.1021/jo00085a004

Reference yield:

: 100-52-7
benzaldehyde

: 1053738-36-5
C₅₆H₆₁Cl₆NO₁₆

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / HCOOH / methanol; H₂O / 21 h / 20 °C

2: 100 percent / K₂CO₃ / tetrahydrofuran / 12 h / Heating

3: 1.) LiN(Si(CH₃)3)2 / 1.) THF, -78 deg C, 1 h, 2.) -78 deg C, 15 min

4: 70 percent / LiOH, H₂O₂ / tetrahydrofuran; H₂O / 15 h / 20 °C

5: 1.) DCC, 2.) DMAP / 1.) toluene, 20 deg C, 5 min, 2.) 20 deg C, 20 h

With dmap; lithium hydroxide; formic acid; dihydrogen peroxide; potassium carbonate; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00085a004