bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

Base Information

Chemical Name:bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate
CAS No.:1323951-98-9
Molecular Formula:C₃₆H₅₆NO₁₄P₅S₅
Molecular Weight:1042.04
Hs Code.:

Synonyms:bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

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Chemical Property of bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

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Technology Process of bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

There total 2 articles about bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1323952-01-7
3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenol

: 2283-11-6
hexaethylphosphoric triamide

: 1323951-98-9
bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

Guidance literature:: 3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenol; hexaethylphosphoric triamide; With triethylamine; In 1,4-dioxane; at 20 ℃; for 360h; Inert atmosphere;

With sulfur; In 1,4-dioxane; for 24h; Inert atmosphere;
DOI:10.1134/S107036321106003X

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 21458-75-3
2-diethylamino-5,5-dimethyl-1,3,2-dioxaphosphorinane

: 1323951-98-9
bis[3,5-bis(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yloxy)phenyl] diethylamidothiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,4-dioxane / 360 h / 50 °C / Inert atmosphere

1.2: 168 h / Inert atmosphere

2.1: triethylamine / 1,4-dioxane / 360 h / 20 °C / Inert atmosphere

2.2: 24 h / Inert atmosphere

With triethylamine; In 1,4-dioxane;
DOI:10.1134/S107036321106003X