4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

Base Information

Chemical Name:4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol
CAS No.:1132675-12-7
Molecular Formula:C₃₁H₃₁BrO₅
Molecular Weight:563.488
Hs Code.:

Synonyms:4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

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Technology Process of 4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

There total 11 articles about 4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 617-86-7
triethylsilane

: 1448000-71-2
1-bromo-4-methoxy-2-(4-(2-methoxy-5-(3-methoxy-4-(methoxymethoxy)styryl)phenoxy)styryl)benzene

: 1132675-12-7
4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

Guidance literature:: With trifluoroacetic acid; at 60 ℃; for 2.5h;
DOI:10.1016/j.tet.2013.06.064

Reference yield: 74.0%

: 1132675-11-6
C₃₃H₃₁BrO₆

: 1132675-12-7
4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

Guidance literature:: With triethylsilane; trifluoroacetic acid; at 60 ℃; for 0.416667h;
DOI:10.1016/j.bmcl.2008.12.022

Reference yield:

: 1448000-67-6
(E)-methyl 3-(4-(2-bromo-5-methoxystyryl)phenoxy)-4-methoxybenzoate

: 1132675-12-7
4-(3-(4-(2-bromo-5-methoxyphenethyl)phenoxy)-4-methoxyphenethyl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.1: toluene / 2 h / 0 °C

3.1: benzene / 24 h / 100 °C

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

4.2: 3 h / 0 °C

5.1: trifluoroacetic acid / 2.5 h / 60 °C

With lithium aluminium tetrahydride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; toluene; benzene; 3.1: |Arbuzov Reaction;
DOI:10.1016/j.tet.2013.06.064