(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

Base Information

Chemical Name:(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone
CAS No.:937174-99-7
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

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Technology Process of (6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

There total 3 articles about (6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 937174-98-6
N-{[2,4-bis(methyloxy)phenyl]methyl}-2-bromo-N-{(2R)-2-hydroxy-3-[(phenylmethyl)oxy]propyl}propanamide

: 937174-99-7
(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 937174-97-5
(S)-1-(benzyloxy)-3-((2,4-dimethoxybenzyl)amino)propan-2-ol

: 937174-99-7
(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran / 16 h / 20 °C

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 20781-20-8
2,4-Dimethoxybenzylamine

: 937174-99-7
(6R)-4-{[2,4-bis(methyloxy)phenyl]methyl}-2-methyl-6-{[(phenylmethyl)oxy]methyl}-3-morpholinone

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 12 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 0 - 20 °C

3: sodium hydride / tetrahydrofuran / 16 h / 20 °C

With sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;