trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile

Base Information

Chemical Name:trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile
CAS No.:95906-30-2
Molecular Formula:C18H23 N
Molecular Weight:0
Hs Code.:2926909090
Mol file:95906-30-2.mol

Synonyms:Benzonitrile,4-[4-(4-pentenyl)cyclohexyl]-, trans-; Benzonitrile,4-[trans-4-(4-pentenyl)cyclohexyl]- (9CI)

Suppliers and Price of trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile

Chemical Property:

PSA：23.79000
LogP:5.18838

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile

There total 7 articles about trans-4-[4-(3-Pentenyl) cyclohexyl] benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 865-47-4
potassium tert-butylate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 101478-52-8
4-[trans-4-(p-cyanophenyl)cyclohexyl]butyraldehyde

: 95906-30-2
p-[trans-4-(4-pentenyl)cyclohexyl]benzonitrile

Guidance literature:: In tert-butyl methyl ether; water; ethyl acetate; Petroleum ether;

Reference yield:

: 1779-49-3
Methyltriphenylphosphonium bromide

: 101478-52-8
4-[trans-4-(p-cyanophenyl)cyclohexyl]butyraldehyde

: 95906-30-2
p-[trans-4-(4-pentenyl)cyclohexyl]benzonitrile

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -20 ℃; for 1.16667h; Yield given;

Reference yield:

: 95925-52-3
p-[4-(methoxymethylene)cyclohexyl]benzonitrile

: 95906-30-2
p-[trans-4-(4-pentenyl)cyclohexyl]benzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 29 percent / 2N HCl / tetrahydrofuran / 0.5 h / Heating

2: 1.) t-BuOK; 2.) 2N HCl / 1.) t-butyl methyl ether, -10 deg C - RT, 165 min; 2.) THF, reflux, 30 min

3: 1.) t-BuOK; 2.) 2N HCl / 1.) t-butyl methyl ether, -10 deg C - RT, 165 min; 2.) THF, reflux, 30 min

4: 1.) t-BuOK; 2.) 2N HCl / 1.) t-butyl methyl ether, -10 deg C - RT, 165 min; 2.) THF, reflux, 30 min

5: 0.8 M n-BuLi / tetrahydrofuran; hexane / 1.17 h / -20 °C

With hydrogenchloride; n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane;