1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride

Base Information

• Chemical Name: 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride
• CAS No.: 1377248-46-8
• Molecular Formula: C₂₁H₂₆N₃O*Cl
• Molecular Weight: 371.91
• Mol file: 1377248-46-8.mol

Synonyms:1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride

Chemical Property of 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride

There total 1 articles about 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) + 2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride (86604-75-3) → 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride (1377248-46-8)

Guidance literature:

2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride; With potassium carbonate; In water; toluene;

N-(2,4,6-trimethylphenyl)imidazole; In toluene; at 110 ℃; for 72h;

DOI:10.1021/om3003027

Reference yield: 77.0%

chloro(dimethylsulfide) gold(I) (29892-37-3) + (Dichloroiodo)benzene (932-72-9) + 1-(2,4,6-trimethylphenyl)-3-((4-methoxy-3,5-dimethyl-)-2-pyridylmethyl)imidazolium chloride (1377248-46-8) → trichloro[1-((4-methoxy-3,5-dimethyl)-2-pyridinylmethyl)-3-(2,4,6-trimethylphenyl)-2H-imidazol-2-ylidene]gold

Guidance literature:

With Ag₂O; In dichloromethane; (Ar) imidazolium salt and Ag2O in CH2Cl2 were stirred at r.t. for 16 h, soln. was filtered through Celite, evapd., react. with (Me2S)AuCl in CH2Cl2 for 24 h, soln. was filtered, evapd., soln. PhICl2 in CH2Cl2 was added at 0°C, overnight at r.t.; solvent was evapd., hexane was added, ppt. was filtered off and dried invacuo; elem. anal.;

DOI:10.1021/om3003027

upstream raw materials:

N-(2,4,6-trimethylphenyl)imidazole

2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride