N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

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Chemical Name:N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide
CAS No.:1440066-28-3
Molecular Formula:C₄₉H₅₀N₂O₆
Molecular Weight:762.946
Hs Code.:

Synonyms:N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

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Chemical Property of N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

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Technology Process of N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

There total 2 articles about N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 875667-84-8
4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine

: 1440066-24-9
C₂₉H₃₂BrNO₄

: 1440066-28-3
N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; for 6h; Inert atmosphere; Reflux;
DOI:10.1016/j.electacta.2013.03.067

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1440066-28-3
N-(1-hexylheptyl)-6-[4-[bis(4-methoxyphenyl)amino]phenyl]anthraquinone-2,3-dicarboxylic imide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol; water / 6 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium carbonate; In tetrahydrofuran; ethanol; water; toluene; 2.1: |Suzuki Coupling;
DOI:10.1016/j.electacta.2013.03.067