[2S-(2α(1R,2S),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

Base Information

Chemical Name:[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine
CAS No.:870298-19-4
Molecular Formula:C₃₀H₄₁NO₃
Molecular Weight:463.66
Hs Code.:

Synonyms:[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

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Chemical Property of [2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

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Technology Process of [2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

There total 1 articles about [2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 824952-29-6
[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-2-[(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy]-1,2-diphenylethanol

: 107-99-3
2-(dimethylamino)ethyl chloride

: 870298-19-4
[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

Guidance literature:: With sodium hydride; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2005.08.030

Reference yield: 89.0%

: 870298-19-4
[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

: 870298-22-9
(1R,2S)-2-(2-dimethylaminoethoxy)-1,2-diphenylethanol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2005.08.030

Reference yield:

: 870298-19-4
[2S-(2α(1R*,2S*),3aα,4β,7β,7aα)]-dimethyl-N-[(2-(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy-1,2-diphenylethoxy)ethyl]amine

: 870298-25-2
oxo-phenylacetic acid (1R,2S)-2-(2-dimethylaminoethoxy)-1,2-diphenylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / p-toluenesulfonic acid / methanol; CH₂Cl₂ / 2 h / 20 °C

2: 80 percent / 2-dimethylaminoisopropyl chloride hydrochloride; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 °C

With dmap; (2-chloropropyl)dimethylamine hydrochloride; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2005.08.030