5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

Base Information

Chemical Name:5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside
CAS No.:339196-22-4
Molecular Formula:C₃₇H₂₈ClF₃N₄O₇S
Molecular Weight:765.166
Hs Code.:

Synonyms:5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

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Technology Process of 5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

There total 9 articles about 5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 421-83-0
trifluoromethane sulfonyl chloride

: 234436-48-7
9-[3-O-benzoyl-5-O-(triphenylmethyl)-β-D-ribofuranosyl]-6-chloro-9H-purine

: 339196-22-4
5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

Guidance literature:: With dmap; In toluene;
DOI:10.1081/NCN-120021951

Reference yield:

: 2004-06-0
6-Chloropurine riboside

: 339196-22-4
5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 38 percent / DMAP / CH₂Cl₂

2.1: pyridine / toluene

2.2: 70 percent / Et₃N / toluene

3.1: 100 percent / DMAP / toluene

With pyridine; dmap; In dichloromethane; toluene;
DOI:10.1081/NCN-120021951

Reference yield:

: 144925-02-0
6-chloro-9-(5′-O-trityl-β-D-ribofuranosyl)purine

: 339196-22-4
5'-O-trityl-3'-O-benzoyl-2'-O-trifluoromethanesulfonyl-6-chloropurine riboside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / toluene

1.2: 70 percent / Et₃N / toluene

2.1: 100 percent / DMAP / toluene

With pyridine; dmap; In toluene;
DOI:10.1081/NCN-120021951