Butyl-p-tolyl-phosphoramidic acid dibutyl ester

Base Information

• Chemical Name: Butyl-p-tolyl-phosphoramidic acid dibutyl ester
• CAS No.: 73732-36-2
• Molecular Formula: C₁₉H₃₄NO₃P
• Molecular Weight: 355.458
• Mol file: 73732-36-2.mol

Synonyms:Butyl-p-tolyl-phosphoramidic acid dibutyl ester

Chemical Property of Butyl-p-tolyl-phosphoramidic acid dibutyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Butyl-p-tolyl-phosphoramidic acid dibutyl ester

There total 3 articles about Butyl-p-tolyl-phosphoramidic acid dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tributyl-N-(p-tolyl)-phosphorimidate (20113-27-3) → Butyl-p-tolyl-phosphoramidic acid dibutyl ester (73732-36-2)

Guidance literature:

With boron trifluoride diethyl etherate; at 60 - 65 ℃;

DOI:10.1007/BF00951895

Reference yield:

tri-n-butyl phosphite (102-85-2) → Butyl-p-tolyl-phosphoramidic acid dibutyl ester (73732-36-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / benzene / 30 - 40 °C

2: 80 percent / Et₂O*BF₃ / 60 - 65 °C

With boron trifluoride diethyl etherate; In benzene;

DOI:10.1007/BF00951895

Reference yield:

p-methylazidobenzene (2101-86-2) → Butyl-p-tolyl-phosphoramidic acid dibutyl ester (73732-36-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / benzene / 30 - 40 °C

2: 80 percent / Et₂O*BF₃ / 60 - 65 °C

With boron trifluoride diethyl etherate; In benzene;

DOI:10.1007/BF00951895

upstream raw materials:

tributyl-N-(p-tolyl)-phosphorimidate

tri-n-butyl phosphite

p-methylazidobenzene