6-(1-cyclohexenyl)caproic acid β-chloroethyl ester

Base Information

• Chemical Name: 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester
• CAS No.: 22354-42-3
• Molecular Formula: C₁₄H₂₃ClO₂
• Molecular Weight: 258.788
• Mol file: 22354-42-3.mol

Synonyms:6-(1-cyclohexenyl)caproic acid β-chloroethyl ester

Chemical Property of 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester

There total 7 articles about 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

1,3-dioxolane-2-spirocyclohexane (177-10-6) → 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester (22354-42-3) + ethylene glycol (107-21-1) + 1,2-dichloro-ethane (107-06-2,52399-93-6) + 2-chloro-ethanol (107-07-3)

Guidance literature:

With hydrogenchloride; at 150 ℃; for 2h;

Reference yield: 8.0%

1,3-dioxolane-2-spirocyclohexane (177-10-6) + 1-(chloromethoxy)butane (2351-69-1) → 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester (22354-42-3)

Guidance literature:

at 130 ℃; for 2h;

Reference yield:

1,3-dioxolane-2-spirocyclohexane (177-10-6) → 6-(1-cyclohexenyl)caproic acid β-chloroethyl ester (22354-42-3)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at 0 ℃;

upstream raw materials:

1,3-dioxolane-2-spirocyclohexane

1,2,2,2-tetrachloroethyl methyl ether

6-Cyclohex-1-enyl-1,4-dioxa-spiro[4.5]decane

6-cyclohex-1-enyl-hexanoic acid ethyl ester