7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one

Base Information

Chemical Name:7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one
CAS No.:86557-23-5
Molecular Formula:C₂₂H₁₈O₃
Molecular Weight:330.383
Hs Code.:
Mol file:86557-23-5.mol

Synonyms:1,2,3,4-Tetrahydro-7-methyl-10-phenyl-5H-benzofuro<6,5-c><2>benzopyran-5-one

Suppliers and Price of 7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one

Chemical Property:

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Technology Process of 7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one

There total 9 articles about 7-methyl-10-phenyl-1,2,3,4-tetrahydro-[1]benzofuro[6,5-c]isochromen-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 86557-21-3
<(2-Benzoyl-7,8,9,10-tetrahydro-4-methyl-6-oxo-6H-dibenzopyran-3-yl)oxy>acetic acid

: 86557-23-5
1,2,3,4-Tetrahydro-7-methyl-10-phenyl-5H-benzofuro<6,5-c><2>benzopyran-5-one

Guidance literature:: With sodium acetate; acetic anhydride; for 3h; Heating;
DOI:10.1016/S0040-4020(01)91891-5

Reference yield: 89.0%

: 4-methyl-3-(2-oxo-2-phenylethoxy)-7,8,9,10-tetrahydro-6H-benzo[c]chromen-6-one

: 86557-23-5
1,2,3,4-Tetrahydro-7-methyl-10-phenyl-5H-benzofuro<6,5-c><2>benzopyran-5-one

Guidance literature:: With sodium hydroxide; In isopropyl alcohol; Heating;
DOI:10.1023/A:1014402906251

Reference yield:

: 55047-37-5
3-Hydroxy-4-methyl-7,8,9,10-tetrahydro-6H-dibenzopyran-6-one

: 86557-23-5
1,2,3,4-Tetrahydro-7-methyl-10-phenyl-5H-benzofuro<6,5-c><2>benzopyran-5-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: K₂CO₃ / acetone / 50 - 56 °C

1.2: 96 percent / acetone / 1 h / Heating

2.1: 89 percent / aq. NaOH / propan-2-ol / Heating

With sodium hydroxide; potassium carbonate; In isopropyl alcohol; acetone; 1.1: Williamson reaction / 1.2: Williamson reaction;
DOI:10.1023/A:1014402906251