diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

Base Information

Chemical Name:diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate
CAS No.:386746-37-8
Molecular Formula:C₂₅H₄₂O₅Si
Molecular Weight:450.691
Hs Code.:

Synonyms:diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

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Technology Process of diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

There total 1 articles about diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 930-68-7
cyclohexenone

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: Sodium; (E)-1-ethoxy-2-ethoxycarbonyl-pent-1-en-4-yn-1-olate

: 386746-37-8
diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h; pH=7;
DOI:10.1021/ol016718g

Reference yield: 89.0%

: 42599-24-6
E-styryl iodide

: 386746-37-8
diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

: C₃₃H₄₈O₅Si

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine; In benzene; Inert atmosphere;
DOI:10.1021/ol202314q

Reference yield: 78.0%

: 557-93-7
2-bromoprop-1-ene

: 386746-37-8
diethyl 1-(3-triisopropylsiloxy-2-cyclohexenyl)-3-butyne-1,1-dicarboxylate

: 1334547-93-1
C₂₈H₄₆O₅Si

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine; In benzene; Inert atmosphere;
DOI:10.1021/ol202314q