Technology Process of N-vinyl-trans-cinnamide
There total 1 articles about N-vinyl-trans-cinnamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine;
In
tetrahydrofuran;
at 50 ℃;
for 17h;
DOI:10.1021/jo050669u
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium (0);
In
1,4-dioxane;
at 85 ℃;
for 1h;
DOI:10.1021/jo050669u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: DIPEA / Pd2(dba)3; 1,1'-bis(diphenylphosphino)ferrocene / dioxane / 1 h / 85 °C
2: 37 mg / hydrogen / Rh(PPh3)3Cl / ethanol; dioxane / 20 °C
With
hydrogen; N-ethyl-N,N-diisopropylamine;
1,1'-bis-(diphenylphosphino)ferrocene; Wilkinson's catalyst; tris(dibenzylideneacetone)dipalladium (0);
In
1,4-dioxane; ethanol;
1: Heck coupling;
DOI:10.1021/jo050669u
