Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)

Base Information

Chemical Name:Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)
CAS No.:95579-22-9
Molecular Formula:C₈H₁₂N₂O₂
Molecular Weight:168.195
Hs Code.:
Mol file:95579-22-9.mol

Synonyms:Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)

Suppliers and Price of Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)

Chemical Property:

PSA：38.50000
LogP:0.60900

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI)

There total 6 articles about Isoxazolo[4,5-c]pyridine, 4,5,6,7-tetrahydro-3-methoxy-5-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 95579-17-2
OMe-THPO

: 95579-22-9
3-Methoxy-5-methyl-4,5,6,7-tetrahydroisoxazolo[4,5-c]pyridine

Guidance literature:: With formic acid; In water; at 100 ℃; for 1h;
DOI:10.1021/jm00156a018

Reference yield:

: 53601-98-2
methyl 3-hydroxy-4,5,6,7-tetrahydroisoxazolo<4,5-c>pyridine-5-carboxylate

: 95579-22-9
3-Methoxy-5-methyl-4,5,6,7-tetrahydroisoxazolo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃ / 1.) acetone, 50 deg C, 1 h, 2.) acetone, 50 deg C, 20 h

2: KOH / methanol; H₂O / 15 h / Heating

3: formic acid / H₂O / 1 h / 100 °C

With potassium hydroxide; formic acid; potassium carbonate; In methanol; water;
DOI:10.1021/jm00156a018

Reference yield:

: 101697-47-6
methyl 3-chloro-4,5,6,7-tetrahydroisoxazolo<4,5-c>pyridine-5-carboxylate

: 95579-22-9
3-Methoxy-5-methyl-4,5,6,7-tetrahydroisoxazolo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol; H₂O / 15 h / Heating

2: formic acid / H₂O / 1 h / 100 °C

With potassium hydroxide; formic acid; In methanol; water;
DOI:10.1021/jm00156a018