Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester

Base Information

• Chemical Name: Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester
• CAS No.: 142502-57-6
• Molecular Formula: C₈H₆F₉IO₂
• Molecular Weight: 432.025
• Mol file: 142502-57-6.mol

Synonyms:Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester

Chemical Property of Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester

There total 1 articles about Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + 1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane (423-39-2) → 3,3,4,4,5,5,6,6,6-Nonafluoro-hexanal (135984-67-7) + Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-hexyl ester (80705-15-3) + Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester (142502-57-6) + 1,4-bis(perflurobutyl)butane-2,3-diol diacetate (80705-16-4)

Guidance literature:

With zinc; In neat (no solvent); at 25 ℃; for 5h; Product distribution; other perfluoroalkyliodides, influence of solvent, size of Zn particles;

DOI:10.1016/S0040-4039(00)92222-6

Reference yield: 91.0%

Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester (142502-57-6) + aniline (62-53-3) + acetone (67-64-1) → 2-perfluoropropyl-6-methyl-N-phenylpyridinium iodide

Guidance literature:

In dichloromethane; Reflux;

DOI:10.3390/molecules24122328

Reference yield: 85.0%

Acetic acid 3,3,4,4,5,5,6,6,6-nonafluoro-1-iodo-hexyl ester (142502-57-6) + aniline (62-53-3) → 3-perfluoropropyl-1-phenylamino-3-phenyliminopropene

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.3390/molecules24122328

upstream raw materials:

vinyl acetate

1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane

Downstream raw materials:

(E)-3-(3-methylphenoxy)-3-perfluoropropyl-prop-2-enal

3-acetoxytoluene

2-methoxyphenyl acetate

Phenyl acetate