C₄₇H₆₄O₉Si

Base Information

• Chemical Name: C₄₇H₆₄O₉Si
• CAS No.: 164530-26-1
• Molecular Formula: C₄₇H₆₄O₉Si
• Molecular Weight: 801.105
• Mol file: 164530-26-1.mol

Synonyms:C₄₇H₆₄O₉Si

Chemical Property of C₄₇H₆₄O₉Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₆₄O₉Si

There total 2 articles about C₄₇H₆₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

C47H63BrO9Si (164530-23-8) → C47H64O9Si + C47H64O9Si (164530-26-1)

Guidance literature:

With chromium dichloride; 1-thiopropane; In dimethyl sulfoxide; at 25 ℃; for 0.5h;

DOI:10.1016/0040-4039(95)00307-X

Reference yield:

C50H71BrO9Si2 (164530-22-7) → C47H64O9Si (164530-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / H₂SiF₆ / acetonitrile / 1.5 h

2: 1-propanethiol, CrCl₂ / dimethylsulfoxide / 0.5 h / 25 °C

With chromium dichloride; fluorosilicic acid; 1-thiopropane; In dimethyl sulfoxide; acetonitrile;

DOI:10.1021/ja9817139

Reference yield: 20.0%

tert-butyldimethylsilyl chloride (18162-48-6) + C47H64O9Si (164530-26-1) → C53H78O9Si2 (223260-54-6) + C53H78O9Si2 (223260-59-1)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; for 5h;

DOI:10.1021/ja9817139

upstream raw materials:

C₄₇H₆₃BrO₉Si

C₅₀H₇₁BrO₉Si₂

Downstream raw materials:

C₅₃H₇₈O₉Si₂

C₅₃H₇₈O₉Si₂