Technology Process of C34H41NO5S
There total 1 articles about C34H41NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-Fmoc-N-Me-Asp(OBn)-OH;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1.58333h;
With
piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
N,N-dimethyl-formamide;
for 3h;
6-(S-tritylmercapto)hexanoic acid;
Further stages;
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1 h
2: trifluoroacetic acid; triphenylmethyl alcohol / dichloromethane / 2.42 h / Inert atmosphere
With
triphenylmethyl alcohol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;