(5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Base Information

• Chemical Name: (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one
• CAS No.: 1164114-99-1
• Molecular Formula: C₃₃H₅₃N₃O₇Si
• Molecular Weight: 631.885

Synonyms:(5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Chemical Property of (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Chemical Property:

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Technology Process of (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

There total 1 articles about (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-azidoethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one (1234579-93-1) → (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one (1164114-99-1)

Guidance literature:

With methanol; trifluoroacetic acid; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol900757k DOI:10.1002/chem.201000104

Reference yield: 93.0%

chloro-trimethyl-silane (75-77-4) + (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-3,4-dihydroxy-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one (1164114-99-1) → (5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)-3,4-bis(trimethylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one (1164115-17-6)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol900757k DOI:10.1002/chem.201000104

upstream raw materials:

(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-azidoethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Downstream raw materials:

(5S,6S)-6-((3R,4R,6R,E)-3-(2-azidoethyl)-7-(4-methoxybenzyloxy)-6-(triisopropylsilyloxy)-3,4-bis(trimethylsilyloxy)hept-1-enyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

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