2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

Base Information

Chemical Name:2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)
CAS No.:1383572-25-5
Molecular Formula:C₂₀H₁₅F₁₂NO₂
Molecular Weight:529.325
Hs Code.:

Synonyms:2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

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Chemical Property of 2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

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Technology Process of 2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

There total 1 articles about 2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 27996-13-0
α,α'-dibromo-di-p-tolylamine

: 684-16-2
Hexafluoroacetone

: 1383572-25-5
2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

Guidance literature:: α,α'-dibromo-di-p-tolylamine; With n-butyllithium; In diethyl ether; at -35 - 20 ℃; for 2h; Inert atmosphere;

Hexafluoroacetone; In diethyl ether; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja302222s

Reference yield: 83.0%

: 62044-68-2
pentabenzyltantalum

: 1383572-25-5
2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

: 1464099-62-4
C₃₄H₂₆F₁₂NO₂Ta

Guidance literature:: In benzene-d6; at 50 ℃; for 16h;
DOI:10.1016/j.poly.2013.07.004

Reference yield:

: 1383572-25-5
2,2'-(azanediylbis(3-methyl-6,1-phenylene))-bis(1,1,1,3,3,3-hexafluoropropan-2-ol)

: 1409972-55-9
C₃₄H₂₉F₁₂NO₂W

Guidance literature:: Multi-step reaction with 3 steps

1: benzene-d6 / 1 h

2: pentane / 4 h

3: diethyl ether

In diethyl ether; benzene-d6; pentane;