C₂₄H₁₉ClF₃N₇O₅S

Base Information

Chemical Name:C₂₄H₁₉ClF₃N₇O₅S
CAS No.:1612242-76-8
Molecular Formula:C₂₄H₁₉ClF₃N₇O₅S
Molecular Weight:609.973
Hs Code.:

C<sub>24</sub>H<sub>19</sub>ClF<sub>3</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂₄H₁₉ClF₃N₇O₅S

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Chemical Property of C₂₄H₁₉ClF₃N₇O₅S

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Technology Process of C₂₄H₁₉ClF₃N₇O₅S

There total 10 articles about C₂₄H₁₉ClF₃N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1612242-74-6
C₂₅H₂₀ClF₃N₆O₆S

: 1612242-76-8
C₂₄H₁₉ClF₃N₇O₅S

Guidance literature:: With ammonia; In methanol; at 20 ℃;

Reference yield:

: 6635-86-5,67476-70-4
2-amino-4-methyl-3-nitropyridine

: 1612242-76-8
C₂₄H₁₉ClF₃N₇O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium nitrite; sulfuric acid / water / 2 h / 0 - 20 °C

2.1: phosphorus(V) oxybromide / 1,2-dichloro-ethane / 12 h / 20 °C / Reflux

3.1: N,N-dimethyl-formamide / 13 h / 100 °C

4.1: sulfuric acid / water / 3 h / 70 °C

5.1: hydrogenchloride; ammonium chloride; iron / water; isopropyl alcohol / Reflux

6.1: 24 h / Reflux

7.1: sulfuric acid; potassium dichromate; Pyrimidin-2(1H)-one / water / 20 - 30 °C

8.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 70 °C

8.2: 70 °C

9.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

9.2: 40 °C

10.1: ammonia / methanol / 20 °C

With Pyrimidin-2(1H)-one; hydrogenchloride; potassium dichromate; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium nitrite; phosphorus(V) oxybromide; In 1-methyl-pyrrolidin-2-one; methanol; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 21901-18-8
4-Methyl-3-nitro-2-pyridone

: 1612242-76-8
C₂₄H₁₉ClF₃N₇O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: phosphorus(V) oxybromide / 1,2-dichloro-ethane / 12 h / 20 °C / Reflux

2.1: N,N-dimethyl-formamide / 13 h / 100 °C

3.1: sulfuric acid / water / 3 h / 70 °C

4.1: hydrogenchloride; ammonium chloride; iron / water; isopropyl alcohol / Reflux

5.1: 24 h / Reflux

6.1: sulfuric acid; potassium dichromate; Pyrimidin-2(1H)-one / water / 20 - 30 °C

7.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 70 °C

7.2: 70 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

8.2: 40 °C

9.1: ammonia / methanol / 20 °C

With Pyrimidin-2(1H)-one; hydrogenchloride; potassium dichromate; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; phosphorus(V) oxybromide; In 1-methyl-pyrrolidin-2-one; methanol; water; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; isopropyl alcohol;