N-(α-Phenylacryloyl)-o-bromanilin

Base Information

Chemical Name:N-(α-Phenylacryloyl)-o-bromanilin
CAS No.:71910-53-7
Molecular Formula:C₁₅H₁₂BrNO
Molecular Weight:302.17
Hs Code.:

Synonyms:N-(α-Phenylacryloyl)-o-bromanilin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(α-Phenylacryloyl)-o-bromanilin

Chemical Property:

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Technology Process of N-(α-Phenylacryloyl)-o-bromanilin

There total 6 articles about N-(α-Phenylacryloyl)-o-bromanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51491-68-0
2-phenylacrylyl chloride

: 615-36-1
2-bromoaniline

: 71910-53-7
N-(α-Phenylacryloyl)-o-bromanilin

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201706325

Reference yield:

: 492-38-6
2-phenylacrylic acid

: 71910-53-7
N-(α-Phenylacryloyl)-o-bromanilin

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere; Sealed tube

With dmap; oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201706325

Reference yield:

: 103-82-2
phenylacetic acid

: 71910-53-7
N-(α-Phenylacryloyl)-o-bromanilin

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 6 h / Reflux

2: potassium carbonate; tetra-(n-butyl)ammonium iodide / toluene / 12 h / 70 °C

3: potassium hydroxide / tetrahydrofuran; water / 2 h / Reflux

4: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 0 - 20 °C

5: triethylamine / dichloromethane / 6 h / 0 - 20 °C

With oxalyl dichloride; sulfuric acid; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c7cc06196j