N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

Base Information

Chemical Name:N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine
CAS No.:181579-49-7
Molecular Formula:C₂₂H₃₀N₄
Molecular Weight:350.507
Hs Code.:

N<sup>2</sup>-(1-Benzyl-piperidin-4-yl)-N<sup>2</sup>-ethyl-N<sup>3</sup>-isopropylidene-pyridine-2,3-diamine

Synonyms:N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

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Technology Process of N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

There total 5 articles about N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 116-11-0
2-Methoxypropene

: 179558-09-9
1-benzyl-4-[N-ethyl-N-(3-amino-2-pyridinyl)amino]piperidine

: 181579-49-7
N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

Guidance literature:: With pyridinium p-toluenesulfonate;
DOI:10.1021/jm960158n

Reference yield:

: 50541-93-0
4-amino-1-benzylpiperidine

: 181579-49-7
N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

2: 84 percent / lithium aluminum hydride / tetrahydrofuran / 16 h / Heating

3: 69 percent / K₂CO₃ / acetonitrile / 72 h / Heating

4: H₂ / platinum oxide / methanol

5: 100 percent / pyridinium p-toluenesulfonic acid

With pyridine; lithium aluminium tetrahydride; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm960158n

Reference yield:

: 50534-23-1
4-acetylamino-1-benzylpiperidine

: 181579-49-7
N²-(1-Benzyl-piperidin-4-yl)-N²-ethyl-N³-isopropylidene-pyridine-2,3-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / lithium aluminum hydride / tetrahydrofuran / 16 h / Heating

2: 69 percent / K₂CO₃ / acetonitrile / 72 h / Heating

3: H₂ / platinum oxide / methanol

4: 100 percent / pyridinium p-toluenesulfonic acid

With lithium aluminium tetrahydride; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/jm960158n