1-(phenylthio)vinyllithium

Base Information

• Chemical Name: 1-(phenylthio)vinyllithium
• CAS No.: 69358-55-0
• Molecular Formula: C₈H₇LiS
• Molecular Weight: 142.151
• Mol file: 69358-55-0.mol

Synonyms:1-(phenylthio)vinyllithium

Chemical Property of 1-(phenylthio)vinyllithium

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(phenylthio)vinyllithium

There total 2 articles about 1-(phenylthio)vinyllithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylthioethylene (1822-73-7) → 1-(phenylthio)vinyllithium (69358-55-0)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Yield given;

DOI:10.1021/jo01313a050

Reference yield:

→ 1-(phenylthio)vinyllithium (69358-55-0)

Guidance literature:

/BRN= 130681/, n-C4H9Li;

Reference yield: 67.0%

1-(phenylthio)vinyllithium (69358-55-0) + methyl iodide (74-88-4) → isopropenyl phenyl sulfide (7594-43-6)

Guidance literature:

DOI:10.1016/S0040-4020(97)00541-3

upstream raw materials:

phenylthioethylene

Downstream raw materials:

phenyl hex-1-en-2-yl sulfide

isopropenyl phenyl sulfide